Column = Vercopak
Inertsil 7 ODS-3 4.6x150mm
Eluent A = 0.1% H3PO4 in H2O
Eluent B = 0.1% H3PO4 and 90% AeCN in H2O
Eluent A/B = 90/10→30 min→0/100%
Flowrate = 1.0ml/min Detection = UV 220nm |
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Peak： |
1.)
6.8 Propionic |
2.) 10.2 n-Butyric |
3.) 13.5 Isopentanoic |
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4.) 14.0 Pentanoic |
5.) 16.3 2-Ethylbutyric |
6.) 17.0 2-Methylpentanoic |
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7.)
17.5 n-Hexanoic |
8.) 20.0 2-Methylhexanoic |
9.) 22.2 2-Ethylhexanoic |
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